Water & Environmental Chemistry Aquacheck Aquacheck Proficiency Testing Scheme Application Form

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Please find below the Aquacheck 2017-2018 distribution schedule. Please complete all the relevant sections of the application form indicating the samples required on pages 2-6 and return to LGC Standards Proficiency Testing by email, fax or post. Returning customer Lab ID: AQ Purchase order no.: (compulsory) Round April 2017-March 2018 Despatch date Reporting Deadline Clean Waters Samples AQ524 24 Apr 22 May 4G 5G 6A 6B 6C 7A 7B 7C 7D 8 8B 9 22 22A 25 26 28 33 37 30 31 Radio Chem Waste Waters AQ525 08 May 05 Jun 1H 1S 2H 2S 2A 3 4 5 5A 5B 5C 36 14 AQ526 30 May 26 Jun 1A 3A 3B 3C 18A 18B 18C 19A 19B 19C 19D 20 20B 21 23 24 27 50 AQ527 12 Jun 10 Jul 10 11 12 12C 15 17A 17B 17C 17D 29 32 13 16 AQ528 26 Jun 24 Jul 4G 5G 6A 6B 6C 7A 7B 7C 7D 8 8B 9 22 25 38 39 40 30 31 AQ529 17 Jul 14 Aug 1H 1S 2H 2S 3 4 5 5B 14 AQ530 31 Jul 29 Aug 1A 3A 3B 3C 18A 18C 19A 19B 19C 19D 20 20B 21 23 24 AQ531 14 Aug 11 Sep 10 11 12 12C 17A 17B 17C 17D 32 35 13 16 AQ532 29 Aug 25 Sep 4G 5G 6A 6B 6C 7A 7B 7C 7D 8 8B 9 22 25 26 28 33 37 30 31 AQ533 11 Sep 09 Oct 1H 1S 2H 2S 2A 3 4 5 5A 5B 5C 36 14 AQ534 25 Sep 23 Oct 1A 3A 3B 3C 18A 18B 18C 19A 19B 19C 19D 20 20B 21 23 24 27 50 AQ535 16 Oct 13 Nov 10 11 12 12C 15 17A 17B 17C 17D 29 32 13 16 AQ536 30 Oct 27 Nov 4G 5G 6A 6B 6C 7A 7B 7C 7D 8 8B 9 22 22A 25 38 39 40 30 31 AQ537 13 Nov 11 Dec 1H 1S 2H 2S 3 4 5 5B 14 AQ538 27 Nov 08 Jan 2018 1A 3A 3B 3C 18A 18C 19A 19B 19C 19D 20 20B 21 23 24 50 AQ539 11 Dec 15 Jan 10 11 12 12C 17A 17B 17C 17D 32 35 13 16 AQ540 15 Jan 2018 12 Feb 4G 5G 6A 6B 6C 7A 7B 7C 7D 8 8B 9 22 22A 25 26 28 33 37 30 31 AQ541 29 Jan 26 Feb 1H 1S 2H 2S 2A 3 4 5 5A 5B 5C 36 14 AQ542 12 Feb 12 Mar 1A 3A 3B 3C 18A 18B 18C 19A 19B 19C 19D 20 20B 21 23 24 27 50 AQ543 26 Feb 26 Mar 10 11 12 12C 15 17A 17B 17C 17D 29 32 13 16 In addition to the above schedule, please note that the Water Framework Directive samples and trial samples are available on page 5. For details on the full technical specification of the scheme please refer to the Aquacheck Scheme Description, which can be downloaded HERE Soils & Sludges Eco tox Page 1 of 6

Please fill in your address details below: Send Test Materials to: Contact name: Department: Company: Address: Town/City: Post/Zip Code: Country: Tel: Fax: E-mail: Send Report Notifications to: Contact name: E-mail*: Send Invoices to: Contact name: Department: Company: Address: Town/City: Post/Zip Code: Country: Tel: Fax: E-mail: VAT no: *An email will be sent to this address to notify when the report is available to download from PORTAL, the online reporting system Please indicate the samples and rounds required on pages 2-6. Sample Clean Waters Inorganic and Nutrients Round number(s) required 1H Major Inorganic Components (Hard Water) 1S Major Inorganic Components (Soft Water) 2H Nutrients and Others (Hard Water) 2S Nutrients and Others (Soft Water) N.B: The per annum discount is applicable for all laboratories taking part in a combination of five rounds of 1H+1S or 2H+2S. 1A Major Ions in Higher Salinity Potable Water 2A ph in Poorly Buffered Waters 3 Non-specific Analytes 3A Inorganic Disinfection By-products 3B Free Chlorine 3C Total Chlorine 4 Metals (Preserved in 0.5% Nitric Acid) 4G Metals in Groundwater (Preserved in 0.5% Nitric Acid) 5 Toxic Metals (Preserved in 0.5% Nitric Acid) 5A Metals for Hydride Generation (Preserved in 0.5% Hydrochloric Acid) 5B EQS Metals (Preserved in 0.5% Nitric Acid) 5C Chromium (VI) in Clean Water 5G Toxic Metals in Groundwater (Preserved in 0.5% Nitric Acid) ***Maximum number of distributions is three. Page 2 of 6

Sample Clean Waters - Organic Round number(s) required 6A Haloforms and Chlorinated Solvents 6B # Phenols 6C # Benzene, Toluene and Xylenes 7A # Organochlorine Pesticides 7B Chlorinated Solvents 7C Polycyclic Aromatic Hydrocarbons 7D Polychlorinated Biphenyls 8 # Acid Herbicides 8B # Triazines and Urea Herbicides 9 # Organophosphorus Pesticides 26 PFOS and PFOA 28 Formaldehyde 33 ## Chlorophyll a 36 ## Taste and Odour 37 ## Acrylamide 38 ## UV Absorbing Organic Constituents 39 ## Geosmin and MIB 40 ## Fungicides Sample Waste Waters and Effluents Inorganic and Nutrients Round number(s) required 10 Nutrients and other analytes 11 Non-specific Analytes 12 # Metals (Preserved in 0.5% Nitric Acid) 12C Chromium (VI) in Waste Water 15 Settleable Solids 29 High and Low COD 35 ## BOD/COD at high concentration Sample Sewage Sludge Inorganic Determinands Round number(s) required 13 Sewage Sludge Inorganics and Specific Elements 16 Compositional Analysis of Sewage Sludge **Maximum number of distributions is two. ***Maximum number of distributions is three. # Please note that certain analytes within these samples are not included in the scope of LGC s UKAS accreditation. Please check the Aquacheck Scheme Description for further details. ## Please note that samples 33-40 are not currently within the scope of LGC s UKAS accreditation. Page 3 of 6

Sample Soils Inorganic Determinands Round number(s) required 14 Agricultural Soil Inorganics and Specific Elements Sample Waste Waters and Effluents Industrial Waste Waters Round number(s) required 17A 17B 17C # 17D 32 ## Sulfide Major Waste Water Analytes Total Phenol, Cyanide and Sulfate Metals (Preserved in 0.5% Nitric Acid) Ammonia, Phosphate and Nitrogen Sample Waste Waters - Organic Round number(s) required 18A 18B # 18C 19A # 19B 19C 19D Haloforms and Chlorinated Solvents Phenols Benzene, Toluene and Xylenes Organochlorine Pesticides Chlorinated Solvents Polycyclic Aromatic Hydrocarbons Polychlorinated Biphenyls 20 # Acid Herbicides 20B # Triazines and Urea Herbicides 21 # Organophosphorus Pesticides 23 Mineral Oil in Water 24 Oil and Grease in Water 27 AOX in Wastewater Sample Qualitative Waters Round number(s) required 22 Qualitative Organics by GCMS 22A Qualitative Organics by Purge and Trap GCMS 25 Qualitative Determination in Clean Water Sample Radiochemistry Round number(s) required 30 Gross Alpha and Gross Beta in Clean Water 31 Aqueous Tritium in Clean Water Sample Ecotoxicology Round number(s) required 50 Ecotoxicology Tests ***Maximum number of distributions is three. ****Maximum number of distributions is four. # Please note that certain analytes within these samples are not included in the scope of LGC s UKAS accreditation. Please check the Aquacheck Scheme Description for further details. ## Please note that sample 32 is not currently within the scope of LGC s UKAS accreditation. Page 4 of 6

Water Framework Directive sample 34 ## Please tick the required samples below. Water & Environmental Chemistry Round Despatch Date Reporting Deadline Samples 34A 34B 34C 34D 34E 34F 34G 34H 34I 34J AQ526 30 May 26 Jun N/A N/A N/A N/A N/A AQ536 30 Oct 27 Nov N/A N/A N/A N/A N/A N/A indicates where samples are unavailable for a particular round. A full description of the samples can be found in the Scheme Description. Aquacheck Trial Samples ## Please indicate the samples required below: Round Despatch Date Reporting Deadline Samples AQ524 24 Apr 22 May Synthetic Pyrethroid Insecticides AQ525 08 May 05 Jun M-Certs AQ526 30 May 26 Jun Triclosan AQ527 12 Jun 10 Jul Haloacetic Acids AQ528 26 Jun 24 Jul Acetate & Iodide (New) AQ529 17 Jul 14 Aug Chelating Agents AQ530 31 Jul 29 Aug Inorganic NPK Fertiliser Bottled Mineral Water (New) AQ531 14 Aug 11 Sep Seawater Nutrients (New) AQ532 29 Aug 25 Sep Semi-Volatile Organic Compounds AQ533 11 Sep 09 Oct Uranium/Plutonium AQ534 25 Sep 23 Oct Organic Fertiliser Swimming Pool Water (New) AQ535 16 Oct 13 Nov Low Level CIP2 contaminants AQ536 30 Oct 27 Nov EQSD Directive Low Level Pesticides (New) AQ537 13 Nov 11 Dec Pharmaceuticals AQ538 27 Nov 08 Jan 2018 M-Certs AQ539 11 Dec 15 Jan Microcystin-LR AQ540 15 Jan 2018 12 Feb Perchlorate AQ541 29 Jan 26 Feb Semi-Volatile Organic Compounds AQ542 12 Feb 12 Mar Seawater Metals (New) AQ543 26 Feb 26 Mar Uranium/Plutonium Sample required (please tick) ## Please note that these samples are not currently within the scope of LGC s UKAS accreditation. The trial samples will be run subject to the registration of a sufficient number of participants. Page 5 of 6

Extra sample costs Full additional samples are available. Please contact LGC Standards Proficiency Testing for the price details For additional waters or spikes please specify your requirements below stating clearly the number of additional samples and the round(s). Please note: Please contact LGC Standards Proficiency Testing for prices. VAT (charged at the prevailing rate) is payable by all participants based in the UK and by those in the rest of the European Union if a VAT Registration Number is not provided. Participants will pay an additional fee to cover courier charges. For details please contact LGC Standards Proficiency Testing. All courier charges set by LGC Standards Proficiency Testing do not include local import charges, taxes (etc.), which must be paid by the participant. Do not send remittance with this form, you will be invoiced subsequently for the full year s participation. No refunds will be given for failure to take part in any round of the PT scheme or for cancellation of rounds that have already been invoiced. LGC Standards Proficiency Testing reserves the right to not send samples or the report for previous samples to any participant that has not paid their subscriptions within the terms stated on the invoice. LGC Standards Proficiency Testing cannot guarantee the number of participants that will return results for any particular parameter in each round. The prices stated are for reporting results and receiving reports electronically via PORTAL (internet reporting). If alternative data entry or reporting methods are required, further charges apply. Please contact LGC Standards Proficiency Testing for the current charges. Aquacheck Trial samples will be run subject to the registration of a sufficient number of participants and LGC Standards Proficiency Testing reserves the right not to provide the samples should they prove technically impractical. By signing this application form, you are agreeing to comply by LGC Standards' Standard Terms and Conditions for the Supply of Laboratory Quality Products and Services. LGC Standards would like to be able to contact you from time to time with information about the LGC Group, its activities, products and services. By completing and returning this form to us, you agree to your personal information being used by LGC Standards and other members of the LGC Group for the administration and provision of our products and services and for related marketing activities. You can change your marketing preferences at any time by emailing askus@lgcgroup.com Signature Date Page 6 of 6