SOIL/SEDIMENT SOIL POWDER

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1 SOIL/ SOIL POWDER Al2O3 CaO CO2 Fe2O3 K2O MgO Na2O P SiO2 TiO2 LOI Ag As Au B Ba Be Bi Br C(org) Others/Set Only Size Type Origin % (0.04)m FeO (4) 100g CRM % m g CRM Ash Sandy % m g CRM Ash Sandy % m g CRM Ash Sandy % m g CRM Red % m g CRM Red % m g CRM Red % m g CRM Grey % m g CRM Grey % m g CRM Grey % m g CRM Black % m g CRM Black % m g CRM Black 071-TILL1 ppm 13.7t 2.72t t 2.15t 2.71t 0.22tm 60.9t 0.98t 7.3t <5 6.4 Acid Leach Data 100g CRM B+C Horizon 071-TILL2 ppm 1.27t 5.39t 3.07t 1.83t 2.19t 0.17tm 60.8t 0.88t 8.1t < g CRM 071-TILL3 ppm 12.2t 2.63t t 1.71t 2.64t 0.11tm 69.1t 0.49t 4.6t < g CRM B+C Horizon 071-TILL4 ppm 1.25t 5.63t 3.25t 1.26t 2.46t 0.2tm 65t 0.81t 5.7t g CRM 202-DC73382 % a n (8.59)a 0.35a 33.5a 50a 590a 2.5a 2.9a -1.8 FeO (1.27) H2O (4.99) 70g CRM 202-DC73383 % a a,n a 13.7a 36a 930a 1.8a 1.2a 4.5a 1.8 FeO (0.56) H2O (2.86) 70g CRM 202-DC73384 % a a,n a 4.4a 23a 1210a 1.4a 0.17a 4.3a 0.49 FeO 0.57 H2O (1.91) 70g CRM 202-DC73385 % a a,n (10.88)a 0.07a 58a 97a 97a 1.85a 1.04a 4a 0.5 FeO 0.5 H2O (10.13) 70g CRM 202-DC73386 % a a,n (9.14)a 4.4a 412a 53a 213a 2a 41a (1.8)a 0.62 FeO (0.22) H2O (8.81) 70g CRM 202-DC73387 % a a,n (10)a 0.2a 220a 57a 118a 4.4a 49a (7.2)a FeO (0.57) H2O (8.9) 70g CRM 202-DC73388 % a n (14.3)a 0.057a 4.8a (10.5)a 180a 2.8a 0.2a 5.2a 0.81 FeO (1.05) H2O (13.73) 70g CRM 202-DC73389 % a a,n a 12.7a 54a 480a 1.9a 0.3a (2.6)a 0.64 FeO (1.2) H2O (3.28) 70g CRM 202-DC77301 % a n 0.067a 2.9a 13.8a 693a 2.1a 0.1a (1.2)a N (0.052) FeO g CRM 202-DC77302 % a n 0.11a 10.5a 38.3a 623a (5)a N (0.012) 50g CRM 202-DC77303 % a n 5.4a 205a 63.9a 550a (3.1)a N (0.32) 50g CRM 202-DC78302 % 7.11n 2.59n 3.34n 2.12n 1.53n 1.52n n a (509)a 2.96a (1.3)a N g+ CRM 262-SOIL7 ppm (4.7)nt (16.3)nt (2.57)nt (1.21)nt (1.31)nt (0.24)nt -460 (18)nt (0.3)nt g CRM % 7.5n 1.89n 3.5n 2.03n 1.51n 1.16n n 0.342n (25 elements) 30g CRM San Joaquin % 6.44n 1.25n 3.38n 2.11n 0.853n 1.14n n 0.283n (25 elements) 30g CRM Montana % 6.53n 2.88n 2.89n 2.45n 1.05n 1.14n n 0.306n (25 elements) 30g CRM

2 SOIL/ SOIL POWDER cont Cd Ce Cl Co Cr Cu Cs Dy Er Eu F Ga Gd Ge Hf Hg Ho I In m TILL TILL TILL < TILL < DC a 70a 66a 14.2a 62a 21a 9a 4.6a 2.6a 1a 506a 19.3a 4.6a 1.34a 6.8a 32a 0.87a 1.9a 0.081a 202-DC a 402a (63)a 8.7a 47a 16.3a 4.9a 4.4a 2.1a 3a 2240a 12a 7.8a 1.2a 5.8a 15a 0.93a 1.8a 0.091a 202-DC a 39a (57)a 5.5a 32a 11.4a 3.2a 2.6a 1.5a 0.72a 246a 13.7a 2.9a 1.17a 6.8a 60a 0.53a 1.3a 0.031a 202-DC a 136a (36)a 22.3a 370a 40.5a 21.4a 6.6a 4.5a 0.85a 540a 30.6a 4.7a 1.91a 14a 590a 1.46a 9.4a 0.12a 202-DC a 91a (78)a 12.3a 118a 144a 15a 3.7a 2.4a 0.82a 603a 31.7a 3.5a 2.6a 8.1a 290a 0.8a 3.8a 4.1a 202-DC a 66a 98a 7.6a 75a 390a 10.8a 3.3a 2.2a 0.66a 906a 29.5a 3.4a 3.2a 7.5a 72a 0.69a 19.4a 0.84a 202-DC a 98a 100a 97a 410a 97a 2.7a 6.6a 2.7a 3.4a 321a 39.3a 9.6a 1.6a 7.7a 61a 1.1a 19.3a 0.1a 202-DC a 66a (68)a 12.7a 68a 24.3a 7.5a 4.8a 2.8a 1.2a 577a 14.8a 5.4a 1.27a 7a 17a 0.97a 1.6a (0.043)a 202-DC a 58.9a (57.4)a 4.9a 26.4a 4.9a 3.3a 3.2a (1.8)a 0.97a 215a 14.6a 3.9a 1.2a 0.015a (0.66)a (0.44)a (0.032)a 202-DC a 76.6a (45.6)a 12.8a 66a 23.2a 7.9a (5.3)a (2.9)a 1.2a 438a 18.8a 5.6a (1.6)a 0.066a (1.1)a (2.6)a (0.07)a 202-DC a 66.3a (101)a 11.6a 59.6a 65.4a 9.3a (4.4)a (2.4)a 1.1a 624a 17.3a 4.6a (1.3)a 0.15a (0.88)a (2.6)a (0.38)a 202-DC a 83.6a 13.1a 60.8a 24.6a (7.3)a (5)a 1.4a (7.3)a (0.018)a 262-SOIL

3 SOIL/ SOIL POWDER cont La Li Lu Mn Mo Nb Nd Ni Pb Pr Rb S Sb Sc Se Sm Sn Sr Ta m m m m m m m m m m m m m TILL tm <0.05t TILL tm <0.05t TILL tm <0.05t < TILL tm t DC a 35.3a 0.41a 1760a 1.4a 16.6a 28a 20.4a 98a 7.5a 140a (310)a 0.87a 11.2a 0.14a 5.2a 6.1a 155a 1.4a 202-DC a 22a 0.32a 510a 0.98a 27a 210a 19.4a 20.2a 57a 88a 210a 1.3a 10.7a 0.16a 18a 3a 187a 0.78a 202-DC a 18.4a 0.29a 304a 0.3a 9.3a 18.4a 12.2a 26a 4.8a 85a 120a 0.45a 5a 0.094a 3.3a 2.5a 380a 0.76a 202-DC a 55.4a 0.75a 1420a 2.6a 37.6a 27.3a 64.2a 58.5a 8.4a 75a 180a 6.3a 20.2a 0.64a 4.4a 5.7a 77a 3.1a 202-DC a 56a 0.42a 1360a 4.6a 24a 24a 40a 552a 7a 117a 410a 35.4a 17.2a 1.56a 4a 17.7a 41.5a 1.8a 202-DC a 36a 0.42a 1450a 18a 26.8a 21a 53a 314a 5.8a 237a 260a 60a 15.5a 1.34a 3.8a 72a 39a 5.3a 202-DC a 19.5a 0.35a 1780a 2.9a 64a 45a 276a 13.6a 11a 15.8a 250a 0.42a 28a 0.32a 10.8a 3.6a 26a 3.9a 202-DC a 35.5a 0.43a 650a 1.16a 15a 32a 31.5a 21a 8.3a 96a 120a 1.04a 11.7a 0.12a 5.9a 2.8a 236a 1.05a 202-DC a 14.3a 0.27a 262a 0.43a 13a 26a 9.3a 16.3a (7.1)a 97.4a (97)a 0.21a 4.8a 4.9a 1.4a 270a 202-DC a 33.2a 0.46a 706a 0.84a 17.1a 34.4a 27.6a 29.2a (8.8)a 109a (174)a 0.93a 11.4a 6.6a 4.2a 188a 202-DC a 29.4a 0.36a 9700a 1.5a 15.1a 27.4a 24.2a 2700a (7.5)a 111a (999)a 9.2a 11a 5.4a 64.3a 130a 202-DC a (0.48)a 677a 42.3a 31.1a 14.2a 135a (0.4)a 10.8a 0.16a 7.1a 163a (1.1)a 262-SOIL

4 SOIL/ SOIL POWDER cont Tb Te Th Tl Tm U V W Y Yb Zn Zr TILL < TILL TILL3 < < TILL DC a (0.051)a 11.6a 1a 0.42a 3.3a 86a 3.1a 25a 2.66a 680a 245a 202-DC a (0.035)a 16.6a 0.62a 0.42a 1.45a 62a 1.08a 21.7a 1.97a 42.3a 219a 202-DC a 0.04a 6a 0.5a 0.28a 1.26a 36.5a 0.95a 15a 1.68a 31.4a 246a 202-DC a (0.15)a 27.3a 0.94a 0.7a 6.7a 247a 6.2a 39a 4.8a 210a 500a 202-DC a (4)a 22.7a 1.6a 0.41a 6.5a 166a 33.5a 21a 2.8a 494a 272a 202-DC a (0.42)a 23a 2.4a 0.4a 6.7a 130a 89.5a 18.8a 2.7a 96.6a 220a 202-DC a (0.047)a 9.1a (0.21)a 0.42a 2.2a 245a 1.23a 26.6a 2.4a 142a 318a 202-DC a 0.046a 11.8a (0.59)a 0.46a 2.7a 81.4a 1.7a 26a 2.8a 68a 229a 202-DC a (0.024)a 8.4a 0.58a 0.28a 1.6a 34.7a 0.98a 16.9a 1.8a 34.2a 300a 202-DC a (0.035)a 12a 0.62a 0.48a 2.4a 82.7a 5a 27.4a 3.1a 72.8a 337a 202-DC a (0.055)a 12.6a (1.7)a 0.4a 3.3a 88.5a 6.9a 24.2a 2.5a 3800a 192a 202-DC78302 (0.9)a 17.6a 3.84a 77.5a 3.1a 58a 262-SOIL

5 SOIL/ SOIL POWDER Al2O3 CaO CO2 Na2O P SiO2 TiO2 As Ba Cd Co Cr Cu Hg Mn Ni Pb Sb V Zn Others/Set Only Size Type Origin ppm Aq Regia (s) 50g CRM Calcareous R ppm Aq Regia (s) 50g CRM Light Sandy R ppm Aq Regia (s) 50g CRM Sewage Amended ppm 50 25g CRM 071-SO2 % 8.07n 1.96n 1.9n n 0.86n 966a 9a 16a 7a 0.082a a 21a 64a 124a Fe 5.56 K g CRM 071-SO3 % 3.06n 14.63n 0.74n n 0.2n 296a 8a 26a 17a 0.017a a 14a 38a 52a Fe 1.51 K g CRM 071-SO4 % 5.46n 1.11n 1n n 0.34n 11a 61a 22a 0.03a a 16a 90a 94a Fe 2.37 K g CRM 188-SMS % 0.49n 9.36a (365)a 0.198a 11.9a 87.4a 21.2a a 910a 40a 18.9a 1.92a (87.5)a 63.7a Sr 107a Fe g CRM City 188-SSP % 6.34n 14a 315a 0.285a 15.6a 75.3a 30.9a a 734a 37.4a 41.3a 2.11a 89.7a 119a Fe 3.73a Sr 274a 50g CRM 188-SVM % 0.692n 13.6a 582a 0.214a 15.4a 79.8a 30a 0.171a 897a 30.8a 19.6a 4.58a 98.3a 88.8a Fe 3.73n Sr 82a 50g CRM SOIL POLLUTED Al Ca CO2 Fe K Mg Na P SiO2 Ti As Ba Cd Ce Cr Cu Hg La Mn Ni Others/Set Only Size Type Origin % a 305a 455a 107a 390a 291a Leach Data. 50g CRM Brick Works % 34.5a 99.3a 132a 1.5a 33.5a PAH's 80g(5) RM Coal Site % 14.9a 118a 71a 0.53a 27a PAH's 80g(5) CRM Gas Works % a a a g CRM Paint % a a a g CRM Paint cont Pb S Sc Se Si Sr V Zn Others/Set Only Size Type Origin a a 345a Leach Data. 50g CRM Brick Works a a 54.6a 456a PAH's 80g(5) RM Coal Site a a 38a 192a PAH's 80g(5) CRM Gas Works g CRM Paint g CRM Paint PCB 2,2,3,3,4,4 Hexachlorobiphenyl 2,2,3,3,4,4,5 Heptachlorobiphenyl 2,2,3,4,5,6 Hexachlorobiphenyl 2,2,3,4,4,5,5 Heptachlorobiphenyl Others/Set Only Size Type Origin mg/kg g CRM Industrial Soi cont 2,2,4,4,5 Pentachlorobiphenyl 2,2,4,4,5,5 Hexachlorobiphenyl 2,3,4,4,5 Pentachlorophenyl 2,3,3,4,4,5 Hexachlorobiphenyl

6 SOIL/ POWDER Al2O3 CaO CO2 Fe2O3 K2O MgO Na2O P2O5 SiO2 TiO2 LOI Ag As Au B Ba Be Cd Co Cr Others/Set Only Size Type Origin % FeO (1.3) 100g CRM Rock Sediment % E FeO (2,2) 100g CRM Rock Sediment % FeO (0.24) 100g CRM Rock Sediment % FeO (1.3) 100g CRM Rock Sediment cont Cu Ga La Li MnO Mo Nb Ni Pb Rb S Sc Sn Sr V Y Yb Zn Zr TOXIC ELEMENTS Al As Cd Co Cr Cu Fe Hg Mn Ni Pb Se V Zn Others/Set Only Size Type Origin 136-HR1 ppm Leachable & Recoverable 100g CRM Humber River 136-SUD1 ppm a Leachable & Recoverable 100g CRM Sudbury 136-TH2 ppm Leachable & Recoverable 100g CRM Toronto Harbour 136-WQB1 ppm Leachable & Recoverable 100g CRM Lake Ontario 136-WQB3 ppm Leachable & Recoverable 100g CRM Hamilton Harbour ESTUARY Al2O3 CaO C Fe2O3 K2O MgO Na2O P2O5 SiO2 TiO2 LOI Ag As Au B Ba Be Cd Co Cr Others/Set Only Size Type Origin 132-MESS3 % n 0.18a 21.2a 2.30a 0.24a 14.4a 1.5a Sb 1.02a Th 0.90a U (4)a 50g CRM A % 2.297n 0.519n 2.008n 0.864n 0.388n 0.741n 0.027n 40n 0.456n 6.23a 0.148a 40.9a 75g CRM cont Cu Hg La Li Mn Mo Nb Ni Pb Rb S Se Sn Sr V Y Yb Zn 132-MESS3 33.9a 0.091a 73.6a 324a 2.78a 46.9a 21.9a a 2.50a 125a 243a A 10.01a 234.5a 11.7a a 44.84a 48.9a HARBOUR Al2O3 CaO C Fe2O3 K2O MgO Na2O P2O5 SiO2 TiO2 LOI Ag As Au B Ba Be Cd Co Cr Others/Set Only Size Type Origin 132-PACS2 % a 26.2a 2.11a 11.5a 90.7a Cl (3) Sb 11.3a 65g CRM cont Cu Hg La Li Mn Mo Nb Ni Pb Rb S Se Sn Sr V Y Yb Zn 132-PACS2 310a 3.04a 32.2a 440a 5.43a 39.5a 183a a 276a 133a 364a LAKE Al2O3 CaO C Fe2O3 K2O MgO Na2O P2O5 SiO2 TiO2 LOI Ag As Au B Ba Be Cd Co Cr Others/Set Only Size Type Origin 071-LKSD1 % (0.6)a (40)a (0.005)a (49)a (430)a (1.1)a (11)a (31)a Br (11)a /Y 100g CRM 071-LKSD2 % (0.8)a (11)a (0.003)a (65)a (780)a (2.5)a (17)a (57)a Br (18)a /Y 100g CRM 071-LKSD3 % (2.7)a (27)a (0.003)a (25)a (680)a (1.9)a (30)a (87)a Br (16)a /Y 100g CRM 071-LKSD4 % (<0.5)a (16)a (0.002)a (22)a (330)a (1)a (11)a (33)a Br (49)a /Y 100g CRM 262-SL1 % 6.74n (1.45)n (0.170)n 0.517n 27.5a 639a (0.26)a 19.8a (104)a Ce 117a Th 14a 25g CRM 262-SL3 % (2.45n) (11.11)n 0.874n (2.7)n (0.669)n (2.61)n 3.2a (1.38)a Br (5.6)a Ce 45.5a Th 7a 25g CRM cont Cu Ga La Li Mn Mo Nb Ni Pb Rb S Sc Sn Sr V Y Yb Zn Zr 071-LKSD1 (44)a (16)a (7)a (700)a (10)a (7)a (16)a (82)a (24)a (9)a (16)a (250)a (50)a (19)a (2)a (331)a (134)a 071-LKSD2 (37)a (68)a (20)a (2020)a (<5)a (8)a (26)a (44)a (85)a (13)a (5)a (220)a (77)a (44)a (4)a (209)a (254)a 071-LKSD3 (35)a (52)a (25)a (1440)a (<5)a (8)a (47)a (29)a (78)a (13)a (3)a (240)a (82)a (30)a (2.7)a (152)a (178)a 071-LKSD4 (31)a (0.26)a (12)a (500)a (<5)a (9)a (31)a (91)a (28)a (7)a (5)a (110)a (49)a (23)a (2)a (194)a (105)a 262-SL1 (30)a (23.7)a 52.6a (44.9)a (37.7)a 113a (17.3)a (80)a 170a (3.42)a 223a 262-SL3 (2.22)a (0.3)a 21.5a 38.8a (3.91)a 0.47a (1.89)a

7 SOIL/ RIVER POWDER Al2O3 CaO CO2 Fe2O3 K2O MgO Na2O P SiO2 Ti LOI Ag As Au B Ba Be Bi Br Cd Others/Set Only Size Type Origin 202-DC78301 % 3.94n 56a 375a (3.5)a 2.45a 50g CRM % 6.11n 2.6n 3.35n 3.97n 2n 1.2n 0.551n n a 23.4a 414a 2.94a 50g RM Buffalo River 202-DC73359 % a a 0.048a 2a 4.6a 950a 3a 0.66a 0.088a FeO g CRM 202-DC73360 % a a 0.066a 6.2a 10.8a 185a 17.1a 1.64a 0.065a Fe g CRM 202-DC73361 % a a 0.59a 18a 33a 1.5a 0.79a 0.1a FeO (0.72) 70g CRM 202-DC73362 % a a 0.084a 19.7a 52a 470a 2.4a 0.64a 0.19a FeO (0.91) 70g CRM 202-DC73363 % a a 0.36a 75a 51a 440a 2.3a 2.4a 0.82a FeO (0.94) 70g CRM 202-DC73364 % a a 0.36a 13.6a 50a 330a 1.7a 5a 0.43a FeO g CRM 202-DC73365 % a a 1.05a 84a 143a 720a 2.7a 0.66a 1.05a FeO g CRM 202-DC73366 % a a 0.062a 2.4a 3.6a 480a 2a 0.19a 0.081a FeO g CRM 202-DC73367 % a a a 8.4a 54a 430a 1.8a 0.42a (1.5)a I (0.61)a FeO g CRM 202-DC73368 % a a a 25a 26a 42a 0.9a 0.38a (2.4)a 0.26a I 1.6a FeO (0.24) 70g CRM 202-DC73369 % a a (3.02)a 3.2a 188a 68a 260a 26a 50a (2.3)a 1.12a Cl 290a I 2a FeO (0.34) 70g CRM 202-DC73370 % a a a 115a 24a 206a 8.2a 10.9a (1.7)a 2.3a Cl (163)a I 1.8a FeO 70g CRM a % (8.2)n (2.2)n (4.5)n (2.5)n (2)n (2)n (27.8)n a (531)a (2.5)a 40g CRM 0.533a % m m FeO (18) 100g CRM % m m FeO (3) 100g CRM % m m FeO (4) 100g CRM 071-STSD1 % (12.3)n (0.4)m (4600)a (<0.5)a (23)a (89)a (630)a (1.6)a (40)a Au (0.008)a 100g CRM 071-STSD2 % (1.6)n (0.3)m (4870)a (0.5)a (42)a (42)a (540)a (5.2)a (4)a Au (0.003)a 100g CRM 071-STSD3 % (8.4)n (0.4)m (4400)a (0.5)a (28)a (82)a (1490)a (2.6)a (24)a Au (0.007)a 100g CRM 071-STSD4 % (4.1)n (0.2)m (4530)a (<0.5)a (15)a (46)a (2000)a (1.7)a (13)a Au (0.004)a 100g CRM cont Ce Co Cr Cu Cs Dy Er Eu F Ga Gd Ge Hf Hg Ho In La Li Lu 202-DC a 90a 53a 0.22a a 13.5a 121a 5.83a 1.31a 8.4a 202-DC a 20.4a 194a 22a 5.1a 4.4a 2.3a 1.8a 870a 23a 6.1a 1.3a 10a 0.018a 0.88a 0.064a 43a 29.6a 0.42a 202-DC a 2.6a 12a 4.9a 16.6a 11a 8.2a 0.49a 1980a 27.4a 9.5a 1.7a 20a 0.04a 2.6a (0.046)a 90a 101a 1.6a 202-DC a 11.7a 87a 177a 7.8a 4a 2.3a 1.3a 345a 15.9a 4.7a 1.3a 6a 0.05a 0.9a 0.09a 39a 33a 0.39a 202-DC a 18a 81a 37a 10a 4.6a 2.4a 1.3a 740a 20.5a 5a 1.4a 5.8a 0.044a 1a 0.058a 40a 51a 0.47a 202-DC a 18.9a 70a 137a 9.4a 5a 2.8a 1.4a 585a 20.3a 6.4a 1.4a 6.5a 0.1a 0.95a 0.13a 46a 45a 0.46a 202-DC a 24.4a 190a 383a 9.1a 3.8a 2.2a 1.5a 690a 16.7a 5.5a 1.3a 4.9a 0.045a 0.76a 0.14a 39a 40a 0.34a 202-DC a 20.8a 122a 38a 5.9a 4.2a 2.3a 1.3a 890a 17.7a 5.8a 1.4a 4.9a 0.053a 0.96a 0.081a 45a 32a 0.39a 202-DC a 3.6a 7.6a 4.1a 3.6a 2.6a 1.8a 0.56a 204a 10.8a 3.5a 0.94a 14.5a 0.042a (0.96)a (0.043)a 30a 13.2a 0.38a 202-DC a 14.4a 85a 32.1a 5.1a 5.1a 2.8a 1.33a 494a 14a 5.5a 1.28a 9.7a a 0.056a 40a 30a 0.45a 202-DC a 15.3a 136a 22.6a 2.3a 2.2a 1.3a 0.47a 149a 6.4a 2.25a 0.4a 1.8a a 0.45a 0.067a 13a 13a 0.19a 202-DC a 8.5a 40a 78.6a 17.4a 7.2a 4.6a 0.6a 1.65E-08a 18.5a 5.9a 1.81a 5.4a a 1.86a 30a 70.6a 0.78a 202-DC a 8.8a 35a 1230a 7.9a 4.8a 3.1a 0.61a 1250a 14.1a 4.4a 1.87a 8.3a a 0.96a 32.7a 39a 0.58a (95)a (19)a 138a 44.1a (5)a (1.5)a (20)a 1.03a (46)a m STSD1 (51)a (17)a (67)a (36)a (1.8)a (5.6)a (1.6)a (950)a (6.1)a (30)a (11)a (0.8)a 071-STSD2 (93)a (19)a (116)a (47)a (12)a (6.5)a (2)a (940)a (5)a (59)a (65)a (0.7)a 071-STSD3 (63)a (16)a (80)a (39)a (5.2)a (5.4)a (1.3)a (850)a (5.1)a (39)a (23)a (0.8)a 071-STSD4 (44)a (13)a (93)a (65)a (93)a (0.38)a (1.2)a (380)a (5.5)a (24)a (14)a (0.5)a

8 SOIL/ RIVER POWDER cont Mn Mo Nb Nd Ni Pb Pr Rb S Sb Sc Se Sm Sn Sr Ta Tb Te Th 202-DC a (32)a 79a 0.39a a 42.9a 150a 3.07a 11.2a 9.07a 202-DC a 0.74a 35a 39a 76a 24.4a 10a 116a 80a 0.22a 15.6a (0.11)a 7.2a 3.1a 525a 3.7a 0.86a 28a 202-DC a 2a 95a 62a 5.5a 32a 18.6a 470a 89a 0.46a 4.4a 0.2a 10.8a 29a 28a 15.3a 1.8a (0.031)a 70a 202-DC a 92a 16a 30a 25.6a 40a 8.3a 79a 192a 5.4a 14.3a 1.06a 5.3a 3.4a 90a 1a 0.7a 0.14a 9.2a 202-DC a 0.86a 18a 32a 40a 30.4a 9.3a 130a 354a 1.84a 15.4a 0.29a 6.2a 4a 142a 1.4a 0.9a (0.08)a 14.6a 202-DC a 1.2a 19a 35a 34a 30a (9.6)a 118a 410a 3.9a 14.5a 0.4a 6.6a 4.6a 204a 1.4a 0.9a (0.12)a 15.2a 202-DC a 7.7a 12a 33a 78a 27a 8.4a 107a 784a 1.25a 17a 0.3a 5.6a 2.8a 266a 0.75a 0.69a (0.14)a 9a 202-DC a 1.4a 17.2a 37a 53a 350a 9.6a 147a 190a 2.6a 14.6a 0.3a 6.1a 5.4a 220a 1.35a 0.76a (0.065)a 12.6a 202-DC a 0.54a 35a 21a 2.7a 21a 5.7a 132a (80)a 0.24a 5.7a (0.15)a 3.8a 9.4a 52a 3.7a 0.54a 13.4a 202-DC a 0.64a 17.7a 34a 32.3a 23a 9.2a 80a 150a 0.81a 11.1a 0.16a 6.3a 2.6a 166a 1.3a 0.87a (0.04)a 202-DC a 1.2a 6.8a 11.8a 30.2a 27a 3.2a 9.2a 90a 6.3a 0.8a 0.28a 2.4a 1.4a 25.3a (0.52)a 0.42a 0.08a 202-DC a 25a 27a 14.3a 636a 7.4a 408a 170a 14.9a 4.1a 0.2a 6.2a 370a 29a 5.7a 1.13a (0.38)a 202-DC a 0.8a 15.4a 25.6a 12.8a 285a 6.9a 270a 940a 24.3a 7.4a 0.25a 5a 54a 24.4a 3.2a 0.82a 0.29a a 42.3a (6)a 15.25a 0.214a (6)a (18)a n n n STSD1 (3950)a (<5)a (5)a (28)a (24)a (35)a (30)a (3.3)a (14)a (6)a (4)a (170)a (0.4)a (1.2)a (3.7)a 071-STSD2 (1060)a (13)a (20)a (43)a (53)a (66)a (104)a (4.8)a (16)a (8)a (5)a (400)a (1.6)a (1.3)a (17.2)a 071-STSD3 (2730)a (6)a (12)a (33)a (30)a (40)a (68)a (4)a (7)a (4)a (230)a (0.9)a (1.1)a (5.5)a 071-STSD4 (1520)a (<5)a (9)a (21)a (30)a (16)a (39)a (7.3)a (14)a (5)a (21)a (350)a (0.6)a (0.9)a (4.3)a cont Tl Tm U V W Y Yb Zn Zr H2O 202-DC78301 (96)a (251)a a 3.09a 94.6a 408a 202-DC a 0.39a 4.4a 121a 1.04a 22a 2.4a 79a 310a DC a 1.55a 17a 16.5a 24.4a 6.7a 11a 44a 460a DC a 0.39a 1.86a 120a 4.9a 22a 2.6a 52a 220a DC a 0.48a 2.6a 118a 2.5a 26a 2.9a 101a 188a DC a 0.48a 2.6a 109a 3.2a 26a 2.9a 243a 220a DC a a 142a 25a 20.2a 2.1a 144a 170a DC a 0.44a 3.5a 96a 5.5a 24a 2.6a 238a 162a DC a 0.33a 3a 26a 2a 18a 2.1a 43a 490a DC a 0.44a 2.6a 97a 1.76a 26.6a 2.8a 78a 370a DC a 0.2a 2.1a 107a 1.63a 13.8a 1.2a 46a 70a DC a 0.74a 9.1a 46.8a 126a 42.7a 5.1a 373a 153a DC a 0.53a 7.8a 46.6a 37.4a 29.3a 3.7a 498a 234a (0.5)a (6)a (105)a 142a STSD1 (8)a (98)a (<4)a (42)a (4)a (198)a (218)a STSD2 (18.6)a (101)a (<7)a (37)a (3.7)a (246)a (185)a STSD3 (10.5)a (134)a (<4)a (36)a (3.4)a (204)a (196)a STSD4 (3)a (106)a (<4)a (24)a (206)a (107)a (190)a -1.73

9 SOIL/ MARINE POWDER Al2O3 CaO CO3 Fe2O3 K2O MgO Na2O P2O5 SiO2 TiO2 LOI Ag As B Ba Cd Cl Ce Co Cr Others/Set Only Size Type Origin 202-DC74301 % (9.93)a 5.8a 125a a 76.7a 58.4a H2O 5.39 C(org) (0.25) FeO (0.29) 25g+ CRM 202-DC75301 % a (73)a 425a 0.2a (78)a (14.2)a 85a C(org) (0.5) 75g CRM Offshore cont Cu Cs Dy Er Eu F Ga Gd Hg Ho La Li Lu MnO Mo Nb Nd Ni Pb 202-DC a 9.4a 19.9a 11a 5.3a a 22a 4.3a 67.8a 60a 1.46a a (15.1)a 91.8a 150a 29.3a 202-DC a (5.4)a (3)a (1.3)a (16.1)a (5.6)a 0.048a (1)a (38)a (0.45)a (0.64)a (19.1)a (33)a 34.3a 25a cont Pr Rb S Sb Sc Se Sm Sr Tb Th Tm U V W Y Yb Zn Zr 202-DC a 97.3a a 25.6a 21.5a 267a 3.4a 13.9a 1.54a 1.98a 112a 5.5a 104a 9.8a 160a 177a 202-DC75301 (8.7)a (109.3)a (1.4)a (12.5)a 16a (6.7)a 150a (0.83)a (10.2)a (0.44)a (2.7)a (103.1)a (2.1)a (27)a (2.8)a 87a (229)a OOZE/SILT Al2O3 CaO CO2 Fe2O3 K2O MgO Na2O P2O5 SiO2 TiO2 LOI Ag As Au B Ba Be Ce Co Cr Others/Set Only Size Type Origin % FeO g CRM Clay % FeO g CRM Volcanogeous % FeO g CRM Calcareous % a U g CRM Siliceous Silt % a U g CRM Clay, deep water cont Cu Ga La Li MnO Mo Ni Pb Rb S Sc Sn Sr Th V Y Yb Zn Zr ORGANIC CONTAMINENT TIN Dibutyltin Tributyl Others/Set Only Size Type Origin µg/kg g CRM Coastal PAH Anthracene Benz(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(ghi)perylene Benzo(k)fluoranthene Fluorthene ndeno(1,2,3-cd)pyrene Others/Set Only Size Type Origin µg/g (PAH) (PCB) (30 elements) 50g CRM cont Perylene Phenanthrene Pyrene

DOE N /29/95 Expires: [1 year after initiation]

DOE N /29/95 Expires: [1 year after initiation] DOE N 441.1 SUBJECT: RADIOLOGICAL PROTECTION FOR DOE ACTIVITIES 9/29/95 Expires: [1 year after initiation] The Department of Energy (DOE) undertook an initiative to reduce the burden of unnecessary, repetitive,